Determination of Yield Stress in Complex Fluids: Theory, Methods and Applications

XU Jia-tong; ZHOU Zi-yu; LIAO Qing-yu; ZHANG Hong-bin

doi:10.14028/j.cnki.1003-3726.2025.24.373

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Determination of Yield Stress in Complex Fluids: Theory, Methods and Applications

更新时间：2025-04-29

- Determination of Yield Stress in Complex Fluids: Theory, Methods and Applications
- Polymer Bulletin Vol. 38, Issue 5, Pages: 689-717(2025)
- 作者机构：
  
  上海交通大学化学化工学院，高分子科学与工程系，流变学研究所，上海 200240
- 作者简介：
- 基金信息：
- DOI：10.14028/j.cnki.1003-3726.2025.24.373
  CLC：
- Received：08 December 2024，
  
  Accepted：2025-01-17，
  
  Published Online：26 March 2025，
  
  Published：20 May 2025
- 稿件说明：
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徐家通, 周子愉, 廖晴雨, 张洪斌. 复杂流体屈服应力的测定: 理论、方法及应用. 高分子通报, 2025, 38(5), 689–717.

Xu, J. T.; Zhou, Z. Y.; Liao, Q. Y.; Zhang, H. B. Determination of yield stress in complex fluids: theory, methods and applications. Polym. Bull. (in Chinese), 2025, 38(5), 689–717.
徐家通, 周子愉, 廖晴雨, 张洪斌. 复杂流体屈服应力的测定: 理论、方法及应用. 高分子通报, 2025, 38(5), 689–717. DOI： 10.14028/j.cnki.1003-3726.2025.24.373.

Xu, J. T.; Zhou, Z. Y.; Liao, Q. Y.; Zhang, H. B. Determination of yield stress in complex fluids: theory, methods and applications. Polym. Bull. (in Chinese), 2025, 38(5), 689–717. DOI： 10.14028/j.cnki.1003-3726.2025.24.373.

摘要

多相多组分复杂流体，因其独特的流变学性质在科学研究和工业应用中占有重要地位。很多高分子的溶液、乳液、悬浮液、凝胶、填充体系等，都是典型的具有屈服行为的复杂流体，也称屈服应力流体。屈服应力是描述这类流体发生固-液转变时的最关键参数，对于理解其流变行为、加工和应用至关重要。尽管屈服应力的研究历史已经有数十年，但迄今仍有许多焦点问题有待解决和深入研究。屈服应力测定的理论、方法和应用场景一直处于不断发展中。特别是对于时间依赖的触变性屈服应力流体，其聚集态形式、热历史及剪切历史均在很大程度上影响其屈服应力的大小，对这类流体屈服应力的准确测定从理论到测试方法都充满挑战。本文综述了屈服应力流体的类别和屈服的形成机制，对现有各类流变模型以及测试方法进行了详细对比分析，还介绍了基于大振幅振荡剪切的应力分叉法和代数应力分叉法这2种屈服应力测定新方法以及二次屈服，着重指出了屈服应力测试中应考虑的科学性、合理性以及时间尺度问题。

Abstract

Multi-phase multi-component complex fluids play an

important role in scientific research and industrial applications due to their unique rheological properties. Many polymer solutions

emulsions

suspensions

gels

filling systems

etc

are typical complex fluids with yield behavior

also known as yield stress fluids. The yield stress is the most critical parameter describing the solid-liquid transition that occurs in these fluids

and it is essential to understand their rheological behavior

processing

and applications. However

despite decades of research on the yield stress

many focal issues still need to be resolved and thoroughly investigated. Theories

methods

and application scenarios for yield stress determination have been constantly being developed. In particular

for time-dependent thixotropic yield stress fluids

the form of the aggregation state

thermal history

and shear history significantly affect the magnitude of the yield stress

and the accurate determination of the yield stress of such fluids is challenging from theory to test methods. In this review

the categories of yield stress fluids and the formation mechanism of yielding are reviewed

the existing rheological models and test methods are analyzed in detail

and the two new methods of yield stress determination of the stress bifurcation method and the algebraic stress bifurcation method based on large-amplitude oscillatory shear are introduced

as well as the secondary yield

which highlights the scientific

rational

and time scale issues that should be considered in the yield stress test.

关键词

Keywords

references

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