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武汉工程大学材料科学与工程学院,武汉 430205
* E-mail:zyf3006@126.com.
纸质出版日期:2021-04-20,
收稿日期:2020-01-15,
修回日期:2020-12-23,
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张云飞, 孙富昌, 郭明明, 杜飞鹏, 郭庆中, 李亮, 鄢国平. 聚乙烯醇导电水凝胶制备的综合实验设计[J]. 高分子通报, 2021,34(4):58-64.
Yun-fei ZHANG, Fu-chang SUN, Ming-ming GUO, Fei-peng DU, Qing-zhong GUO, Liang LI, Guo-ping YAN. Design of a Comprehensive Experiment for Preparation of Polyvinyl Alcohol Conductive Hydrogels[J]. Polymer Bulletin, 2021,34(4):58-64.
张云飞, 孙富昌, 郭明明, 杜飞鹏, 郭庆中, 李亮, 鄢国平. 聚乙烯醇导电水凝胶制备的综合实验设计[J]. 高分子通报, 2021,34(4):58-64. DOI: 10.14028/j.cnki.1003-3726.2021.04.008.
Yun-fei ZHANG, Fu-chang SUN, Ming-ming GUO, Fei-peng DU, Qing-zhong GUO, Liang LI, Guo-ping YAN. Design of a Comprehensive Experiment for Preparation of Polyvinyl Alcohol Conductive Hydrogels[J]. Polymer Bulletin, 2021,34(4):58-64. DOI: 10.14028/j.cnki.1003-3726.2021.04.008.
设计了聚乙烯醇(PVA)导电水凝胶制备的综合实验。实验设计包括:前期文献调研、聚3
4-乙撑二氧噻吩/聚苯乙烯磺酸盐(PEDOT∶PSS)掺杂PVA 水凝胶(PEDOT∶PSS/PVA)的制备、水凝胶结构表征与性能测试等部分。采用傅里叶变换红外光谱、扫描电子显微镜分别表征了PEDOT∶PSS/PVA的组成与形貌;采用数字万用表表征了PEDOT∶PSS/PVA 的电导率;采用电子万能试验机表征了PEDOT∶PSS/PVA 的机械性能及力敏性能。数据表明:PEDOT∶PSS/PVA具有良好的机械性能、导电性及力敏性能
且随着PEDOT∶PSS掺杂量的增加
PEDOT∶PSS/PVA的导电性、机械性能及力敏性能有所增加。教学实践表明
综合实验的开展有利于提高学生综合运用材料、化学专业知识的能力
在锻炼学生动手能力的同时
培养其分析问题、解决问题的能力。
A comprehensive experiment of preparation of polyvinyl alcohol (PVA) based conductive hydrogel is designed. The experimental design includes the preliminary investigation
the preparation of poly (3
4- ethylenedioxythiophene)/poly(styrenesulfonate) (PEDOT∶PSS) doped PVA hydrogels (PEDOT∶PSS/PVA)
structure characterization and performance test. The composition and morphology of PEDOT∶PSS/PVA were characterized by Fourier transform infrared spectroscopy (FTIR) and scanning electron microscope (SEM)
respectively. The conductivity of PEDOT∶PSS/PVA was characterized by digital multimeter
and the mechanical properties and strain sensitivity of PEDOT∶PSS/PVA were characterized by universal tensile machine. The results showed that the PEDOT∶PSS/PVA had good mechanical properties
electrical conductivity and strain sensitivity. With the increase of PEDOT∶PSS doping
mechanical properties
the electrical conductivity and strain sensitivity of PEDOT∶PSS/PVA increased. The teaching practice has shown that the designed comprehensive experiment is beneficial for improving students’ ability to comprehensively apply materials and chemistry knowledge
as well as students’ ability to analyze and solve problems besides operational skills.
PEDOT∶PSS/PVA机械性能导电性能力敏性能实验设计
PEDOTPSS/PVAMechanical propertiesConductivityStrain sensitivityExperiment design
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