Xiao WANG, Xue WU, Chun ZHAO. Effect of Enzyme Pretreatment Combined with High Pressure Jet on Physicochemical Properties of Microfibrillated Cellulose[J]. Polymer Bulletin, 2022,35(9):52-59.
Xiao WANG, Xue WU, Chun ZHAO. Effect of Enzyme Pretreatment Combined with High Pressure Jet on Physicochemical Properties of Microfibrillated Cellulose[J]. Polymer Bulletin, 2022,35(9):52-59. DOI: 10.14028/j.cnki.1003-3726.2022.09.007.
Cellulase pretreatment has attracted much attention in the preparation of microfibrillated cellulose due to its environmental friendliness. In this study
different concentrations of cellulase and high pressure jet treatment were used to prepare microfibrillated cellulose. The results show that the diameter of cellulose fibrils was decreased from several or tens of microns to tens or hundreds of nanometers and crystal structure was not changed after cellulase pretreatment and high pressure jet treatment. The particle size analysis shows that the cellulose micronizing level based on 1% (w/w ) cellulase pretreatment and high pressure jet treatment is higher. With the increase of enzyme concentration from 0.1% to 0.5%
the viscosity of cellulose aqueous dispersion increased
and the thermal stability and the tensile properties of cellulose films were enhanced. The average tensile strength of the films treated with 0.5% enzyme and high pressure jet treatment is 18.74MPa. The tensile properties of the films treated with 1% cellulase pretreatment and high pressure jet treatment had little change. And the average tensile strength is 18.99MPa