Experimental teaching plays a very important role in polymer material science. A new characteristics experiment about polymer resin synthesis technology was designed based on the comprehensive experimental teaching system for senior students majoring in polymers. The characteristics experiment focused on the synthesis and characterization of ablation resistive phenolic resin. The professional characteristic of the new experimental teaching contents is distinctive. The professional skills and the ability of innovative and scientific research of the senior students could be improved effectively

which will promote the goal achievement of talent cultivation.